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Setup List
Holder Status Name ExpNo Experiment User Time Title
12 Completed warren-viii-67 aliquot 400 10 N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) Speed 00:01:24 post condensation, pre-acylation
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
12 11:49:56 warren-viii-67 aliquot 400 10 1d_1H_HSolv Speed + + - + + + - post condensation, pre-acylation
11 11:43:59 warren-viii-66 aliquot 400 10 1d_1H_HSolv Speed + + - + + + + post condensation, pre-acylation
5 11:21:16 warren-viii-65 400 1 1d_1H_Dsolv Speed + + - + + + +
4 11:15:27 warren-viii-67 aliquot 400 1 1d_1H_HSolv Speed + + - + + + +
3 11:09:13 warren-viii-66 aliquot 400 1 1d_1H_HSolv Speed + + - + + + +
43 11:00:45 WB_Legacy_83316 2 1d_31P{1H} Battery + - - + + + +
42 10:58:12 WB_Legacy_54273 2 1d_31P{1H} Battery + - - + + + +
25 10:55:36 WB_Legacy_243380 1 1d_31P{1H} Battery + - - + + + + pp: Cannot find any peak for scaling in M:/data/Battery/nmr/WB_Legacy_243380/1/pdata/1/peaks!
48 10:52:58 WB_Legacy_243378 1 1d_31P{1H} Battery + - - + + + +
47 10:50:24 WB_Legacy_243367 1 1d_31P{1H} Battery + - - + + + +
46 10:47:46 WB_Legacy_182434 1 1d_31P{1H} Battery + - - + + + +
45 10:45:09 WB_Legacy_143948 1 1d_31P{1H} Battery + - - + + + +
44 10:42:43 WB_Legacy_141191 1 1d_31P{1H} Battery + - - + + + +
43 10:39:24 WB_Legacy_83316 1 1d_31P{1H} Battery + - - + + + +
42 10:36:53 WB_Legacy_54273 1 1d_31P{1H} Battery + - - + + + +
15 10:35:25 Burke-xi-76 al 3 1d_31P{1H} Speed - - - - - + +
15 10:33:14 Burke-xi-76 al 2 1d_31P{1H} Speed - + - - - + +
15 10:27:02 Burke-xi-76 al 1 1d_1H_HSolv Speed + + - + + + +
14 10:22:09 MF259-5-16-py 2 1d_1H_HSolv Chitnis - + - - - + +
14 10:10:33 MF259-5-16-py 1 1d_31P{1H} Chitnis + + - + + + +
32 10:02:51 EE-2-2 CDCl2 PNMR 30.04.2025 400MHz 1 1d_31P{1H} Stradiotto + + - + + + + EE-2-2 CDCl2 PNMR 30.04.2025 400MHz
38 09:52:25 AN_104_Pyridine_overnight 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+PPDC(10:1)_overnight@115
38 09:46:23 AN_104_Pyridine_overnight 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+PPDC(10:1)_overnight@115 lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
37 09:44:10 AN_105_Dioxane_overnight 2 1d_31P{1H} Chitnis - + - - - + + AN_095+PNBPA@115deg
37 09:37:03 AN_105_Dioxane_overnight 1 1d_1H_HSolv Chitnis + + - + + + + AN_095+PNBPA@115deg
36 09:34:52 AN_103_Pyridine_overnight 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+PPDC(1:10)_overnight@115
36 09:28:52 AN_103_Pyridine_overnight 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+PPDC(1:10)_overnight@115 lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
35 09:26:43 AN_102_pyridine_overight 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+PPDC(1:1)_overnight @115
35 09:19:46 AN_102_pyridine_overight 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+PPDC(1:1)_overnight @115
9 21:09:09 CO_230 pH 10.12 16 1d_water Jakeman - - - - - + + CO_230 pH 10.12
9 19:40:19 CO_230 pH 10.12 15 1d_13C_UDEFT Jakeman + - - + + + + CO_230 pH 10.12 loopadj: Loop Filter = 90 Loop Gain = -3.88 Loop Time = 0.32
8 19:30:29 CO_230 pH 1.5 4 1d_water Jakeman - - - - - + + CO_230 pH 1.5
8 18:00:07 CO_230 pH 1.5 3 1d_13C_UDEFT Jakeman + + - + + + + CO_230 pH 1.5 loopadj: Loop Filter = 57 Loop Gain = -7.79 Loop Time = 0.42, pp: Unable to assign a peak for scaling of M:/data/Jakeman/nmr/CO_230 pH 1.5/3/pdata/1/peaks No peak is found in the specified ranges!
40 15:28:11 BM-R3.1b-wet-CDCl3 1 1d_1H_Dsolv Baker + + - + + + +
28 15:22:02 JN-PhNHNa-THF-Apr-29 1 1d_1H_HSolv Chitnis + + - + + + + Aniline + NaTBuO in THF stirred at RT for 30 min Light yellow mixture
2 15:15:17 Burke-xi-74b WU 1 1d_1H_Dsolv Speed + - - + + + +
1 15:08:16 Burke-xi-74a WU 1 1d_1H_Dsolv Speed + + - + + + +
17 14:38:05 AN_104_Pyridine_0time 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+Phenyl phosphorous dichloride(10:1)_0time
17 14:33:07 AN_104_Pyridine_0time 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+Phenyl phosphorous dichloride(10:1)_0time lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
16 14:30:57 AN_103_Pyridine_0time 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+Phenyl phosphorous dichloride(1:10)_0time
16 14:26:05 AN_103_Pyridine_0time 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+Phenyl phosphorous dichloride(1:10)_0time lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
14 14:20:48 JF-25-036 purfied product (Apr 29) 2 1d_13C{1H} Charron - - - - - + +
14 14:13:35 JF-25-036 purfied product (Apr 29) 1 1d_1H_Dsolv Charron + - - + + + +
20 13:55:48 AP-25-015-02 2 1d_13C{1H} Charron - + - - - + +
20 13:48:45 AP-25-015-02 1 1d_1H_Dsolv Charron + + - + + + +
11 13:44:58 AN_102_Pyridine_0time(1) 2 1d_1H_HSolv Chitnis - + - - - + + PNBP+Phenyl phosphorous dichloride_(1:1)_0time lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
11 13:35:50 AN_102_Pyridine_0time(1) 1 1d_31P{1H} Chitnis + + - + + + + PNBP+Phenyl phosphorous dichloride_(1:1)_0time
13 13:29:28 AP-25-016-02 2 1d_13C{1H} Charron - + - - - + +
13 13:21:58 AP-25-016-02 1 1d_1H_Dsolv Charron + + - + + + +
10 13:16:11 aa46 1 1d_1H_Dsolv Jakeman + + - + + + +
9 13:08:04 CO_230 pH 10.12 14 1d_11B{1H} Jakeman - - - - - + + CO_230 pH 10.12
9 12:57:49 CO_230 pH 10.12 13 1d_1H_Dsolv Jakeman + - - + + + + CO_230 pH 10.12
8 12:48:23 CO_230 pH 1.5 2 1d_11B{1H} Jakeman - + - - - + + CO_230 pH 1.5
8 12:37:17 CO_230 pH 1.5 1 1d_1H_Dsolv Jakeman + + - + + + + CO_230 pH 1.5
19 12:35:02 AN_087_Pyridine_29.04.2025 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+1,10 DCA pp: Cannot find any peak for scaling in M:/data/Chitnis/nmr/AN_087_Pyridine_29.04.2025/2/pdata/1/peaks!
19 12:31:49 AN_087_Pyridine_29.04.2025 1 1d_1H_HSolv Chitnis + + - + x x - PNBPA+1,10 DCA topshim: TopshimRawCheck - no signal at all TopShim1D::performShimming - MapMeasure1D::checkData line 387: TopshimRawCheck failed; lctshim.ml: Error executing 'topshim lockoff 1h fastfine ordmax=5 o1p=8.253 selwid=0.5 ', Shim failed, pulsecal: no peak found in expected region actual pulse might be significantly shorter than value in prosol table, Acquisition Failed
18 12:29:42 AN_102_pyridine_0time 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+Phenyl phosphorous dichloride(1:1) 0time
18 12:23:47 AN_102_pyridine_0time 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+Phenyl phosphorous dichloride(1:1) 0time lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
17 12:21:37 Burke-xi-74b 13 1d_31P{1H} Speed - + - - - + +
17 12:15:37 Burke-xi-74b 12 1d_1H_HSolv Speed + + - + + + +
16 12:13:17 Burke-xi-74a 2 1d_31P{1H} Speed - + - - - + +
16 12:07:02 Burke-xi-74a 1 1d_1H_HSolv Speed + + - + + + +
15 12:06:09 Burke-xi-73 5 1d_19F{1H} Speed - - - - - + +
15 12:04:06 Burke-xi-73 4 1d_19F{1H} Speed - + - - - + +
15 12:03:06 Burke-xi-73 3 1d_31P{1H} Speed - - - - - + +
15 12:00:45 Burke-xi-73 2 1d_31P{1H} Speed - + - - - + +
15 11:54:07 Burke-xi-73 1 1d_1H_HSolv Speed + + - + + + +
51 11:44:06 PT-051-1d50-P4+BA-NEt3 1 1d_31P{1H} Chitnis + - - + + + + clear colourless sol, white solid
50 11:39:01 PT-050-1d50-P4-NEt3 1 1d_31P{1H} Chitnis + + - + + + + clear colourless sol, white solid
49 11:32:58 PT-049-1d50-BAAz-NEt3 1 1d_1H_HSolv Chitnis + + - + + + + colourless sol, white thing floating
58 11:17:20 AN_098_Dioxane_overnight 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+CDI(1:1)+NaOtBu
58 11:10:18 AN_098_Dioxane_overnight 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+CDI(1:1)+NaOtBu
57 11:08:02 AN_095_Dioxane_overnight 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+CDI (1:2) in dioxane @100 ovrnight
57 11:00:54 AN_095_Dioxane_overnight 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+CDI (1:2) in dioxane @100 ovrnight
56 10:58:40 AN_101_pyridine_0time 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+phenylphosphorousdichloride(3:1)
56 10:52:54 AN_101_pyridine_0time 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+phenylphosphorousdichloride(3:1) lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
55 10:50:41 AN_100_Pyridine_0time 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+phenylphosphorousdichloride(1:3)
55 10:44:56 AN_100_Pyridine_0time 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+phenylphosphorousdichloride(1:3) lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
54 10:42:33 AN_099_0time_pyridine 2 1d_31P{1H} Chitnis - + - - - + + PNBPA+phenylphosphorousdichloride(1:1)
54 10:36:31 AN_099_0time_pyridine 1 1d_1H_HSolv Chitnis + + - + + + + PNBPA+phenylphosphorousdichloride(1:1) lclpfilter.ml: freqlist: File not found, Cannot open File not found for reading. Frequency list not found.
31 10:31:13 JN-56-180C-4days-ODCB-Apr-29 3 1d_1H_HSolv Chitnis - + - - - + + P2(NMe)4N(Ph) + P2(NMe)4N(C6F5) in ODCB Heated at 180C for 4 days CC mixture
31 10:26:58 JN-56-180C-4days-ODCB-Apr-29 2 1d_19F{1H} Chitnis - + - - - + + P2(NMe)4N(Ph) + P2(NMe)4N(C6F5) in ODCB Heated at 180C for 4 days CC mixture
31 10:22:22 JN-56-180C-4days-ODCB-Apr-29 1 1d_31P{1H} Chitnis + - - + + + + P2(NMe)4N(Ph) + P2(NMe)4N(C6F5) in ODCB Heated at 180C for 4 days CC mixture
4 09:53:43 Burke-xi-75 al 3 1d_31P{1H} Speed - - - - - + +
4 09:51:25 Burke-xi-75 al 2 1d_31P{1H} Speed - + - - - + +
4 09:44:52 Burke-xi-75 al 1 1d_1H_HSolv Speed + + - + + + +