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Day Experiments: 00:20
Busy Until: Tue 19:03
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
2 Completed KR012825 collagen peptides 10 N 1d_water Water Suppression Experiment (Suppresses Tallest Signal in your Spectrum) Infusd 00:09:14
5 Completed MAL-447-Aliquot-5h 1 N 1d_31P{1H} 31P Observe with 1H Decoupling MacDonald 00:05:37 Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
5 Completed MAL-447-Aliquot-5h 2 N 1d_19F{1H} 19F Observe with 1H Decoupling MacDonald 00:02:48 Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
5 Completed MAL-447-Aliquot-5h 3 N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) MacDonald 00:01:24 Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
6 Completed Muise-ii-34a-1hr run al 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Speed 00:01:30
6 Completed Muise-ii-34a-1hr run al 2 N 1d_31P{1H} 31P Observe with 1H Decoupling Speed 00:02:54
7 Completed MM-078-Sb(NMe2)3 + PFA tol 10min rt 3 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Chitnis 00:01:30
7 Completed MM-078-Sb(NMe2)3 + PFA tol 10min rt 4 N 1d_19F{1H} 19F Observe with 1H Decoupling Chitnis 00:01:29
8 Completed MM-079-PFA+2buli+SbCl3 rt tol 10min 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Chitnis 00:01:30
8 Completed MM-079-PFA+2buli+SbCl3 rt tol 10min 2 N 1d_19F{1H} 19F Observe with 1H Decoupling Chitnis 00:01:29
13 Completed JT-chlorosilane synthesis 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Turculet 00:02:51
13 Completed JT-chlorosilane synthesis 2 N 1d_31P{1H} 31P Observe with 1H Decoupling Turculet 00:00:51
15 Completed jan 28 2025 R-3,4-diCl-MA purity 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Bearne 00:05:31
16 Completed EXP-295 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Bearne 00:01:30
16 Completed EXP-295 2 N 1d_13C{1H} 13C Observe with 1H Decoupling Bearne 00:19:59
16 Running EXP-295 3 N 1d_13C_DEPT 13C DEPT-135 CH3/CH + and CH2 - (USE NS = 4*n) Bearne 00:15:43
30 Submitted SAM-7-080A (with FB) 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Dasog 00:01:30
30 Submitted SAM-7-080A (with FB) 2 N 1d_19F{1H} 19F Observe with 1H Decoupling Dasog 00:01:18
31 Submitted SAM-7-080B (with FB) 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Dasog 00:01:30
31 Submitted SAM-7-080B (with FB) 2 N 1d_19F{1H} 19F Observe with 1H Decoupling Dasog 00:01:18
32 Submitted SAM-7-079B (with FB) 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Dasog 00:01:30
32 Submitted SAM-7-079B (with FB) 2 N 1d_19F{1H} 19F Observe with 1H Decoupling Dasog 00:01:18
41 Completed JH-1-9-Ring5th 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Turculet 00:01:30
48 Completed JF-25-007 DMS-D6 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Charron 00:01:30
48 Completed JF-25-007 DMS-D6 2 N 1d_13C{1H} 13C Observe with 1H Decoupling Charron 00:05:07
50 Completed TOC05 1 N 1d_31P{1H} 31P Observe with 1H Decoupling MacDonald 00:02:54 TOC05 31P{1H} unlock Tol P(I) with S8
50 Completed TOC05 2 N 1d_31P{1H} 31P Observe with 1H Decoupling MacDonald 00:00:48 TOC05 31P{1H} unlock Tol wide P(I) with S8
51 Completed TJH-719-P2N2+ P(NMe2)3 in et3n 2 hrs 65 C 1 N 1d_31P{1H} 31P Observe with 1H Decoupling Chitnis 00:01:32
52 Completed TJH-721-P2N2SP + KHMDS 1 N 1d_31P{1H} 31P Observe with 1H Decoupling Chitnis 00:01:32
53 Completed TJH-722-P2N2SP + TMSOTf 1 N 1d_31P{1H} 31P Observe with 1H Decoupling Chitnis 00:02:54
53 Completed TJH-722-P2N2SP + TMSOTf 2 N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) Chitnis 00:02:20
53 Completed TJH-722-P2N2SP + TMSOTf 3 N 1d_19F{1H} 19F Observe with 1H Decoupling Chitnis 00:00:49
55 Completed TJH-720-P2N2 + Bi crude 1 N 1d_31P{1H} 31P Observe with 1H Decoupling Chitnis 00:01:32
57 Completed JF-25-006 DMSO-D6 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Charron 00:01:30
57 Completed JF-25-006 DMSO-D6 2 N 1d_13C{1H} 13C Observe with 1H Decoupling Charron 00:05:07
58 Completed EBC-69-F2-5 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Thompson 00:01:30
59 Completed EBC-68-crude2 1 N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) Thompson 00:01:30
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
16 18:24:37 EXP-295 3 1d_13C_DEPT Bearne - - - - - - -
16 18:02:59 EXP-295 2 1d_13C{1H} Bearne - + - - - + +
16 17:55:37 EXP-295 1 1d_1H_Dsolv Bearne + + - + + + +
15 17:45:31 jan 28 2025 R-3,4-diCl-MA purity 1 1d_1H_Dsolv Bearne + + - + + + +
13 17:37:37 JT-chlorosilane synthesis 2 1d_31P{1H} Turculet - + - - - + +
13 17:29:41 JT-chlorosilane synthesis 1 1d_1H_Dsolv Turculet + + - + + + +
8 17:25:07 MM-079-PFA+2buli+SbCl3 rt tol 10min 2 1d_19F{1H} Chitnis - - - - - + +
8 17:21:20 MM-079-PFA+2buli+SbCl3 rt tol 10min 1 1d_1H_Dsolv Chitnis + - - + + + +
7 17:16:30 MM-078-Sb(NMe2)3 + PFA tol 10min rt 4 1d_19F{1H} Chitnis - + - - - + +
7 17:11:38 MM-078-Sb(NMe2)3 + PFA tol 10min rt 3 1d_1H_Dsolv Chitnis + + - + + + +
6 17:06:56 Muise-ii-34a-1hr run al 2 1d_31P{1H} Speed - + - - - + +
6 16:59:37 Muise-ii-34a-1hr run al 1 1d_1H_Dsolv Speed + + - + + + +
5 16:54:30 MAL-447-Aliquot-5h 3 1d_1H_HSolv MacDonald - + - - - + + Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
5 16:50:19 MAL-447-Aliquot-5h 2 1d_19F{1H} MacDonald - + - - - + + Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
5 16:42:46 MAL-447-Aliquot-5h 1 1d_31P{1H} MacDonald + - - + + + + Aliquot from reaction of PhPCl2 + ochloranil + NaO2CCF3 in DCM/MeCN cloudly colourless (slighty pale yellow?) mixture
2 16:29:43 KR012825 collagen peptides 10 1d_water Infusd + + - + + + +
59 16:22:47 EBC-68-crude2 1 1d_1H_Dsolv Thompson + - - + + + +
58 16:15:05 EBC-69-F2-5 1 1d_1H_Dsolv Thompson + + - + + + +
55 16:08:24 TJH-720-P2N2 + Bi crude 1 1d_31P{1H} Chitnis + + - + + + +
41 16:01:36 JH-1-9-Ring5th 1 1d_1H_Dsolv Turculet + + - + + + +
53 15:46:18 TJH-722-P2N2SP + TMSOTf 3 1d_19F{1H} Chitnis - + - - - + +
53 15:40:08 TJH-722-P2N2SP + TMSOTf 2 1d_1H_HSolv Chitnis - + - - - + +
53 15:35:35 TJH-722-P2N2SP + TMSOTf 1 1d_31P{1H} Chitnis + - - + + + +
53 15:09:21 TJH-722-P2N2SP + TMSOTf 1 1d_31P{1H} Chitnis + - - + + + +
52 15:06:07 TJH-721-P2N2SP + KHMDS 1 1d_31P{1H} Chitnis + - - + + + +
51 14:30:38 TJH-719-P2N2+ P(NMe2)3 in et3n 2 hrs 65 C 1 1d_31P{1H} Chitnis + - - + + + +
50 14:29:40 TOC05 2 1d_31P{1H} MacDonald - - - - - + + TOC05 31P{1H} unlock Tol wide P(I) with S8
50 14:23:35 TOC05 1 1d_31P{1H} MacDonald + + - + + + + TOC05 31P{1H} unlock Tol P(I) with S8
57 14:18:17 JF-25-006 DMSO-D6 2 1d_13C{1H} Charron - - - - - + + pp: Unable to assign a peak for scaling of M:/data/Charron/nmr/JF-25-006 DMSO-D6/2/pdata/1/peaks No peak is found in the specified ranges!
57 14:11:38 JF-25-006 DMSO-D6 1 1d_1H_Dsolv Charron + - - + + + +
48 14:05:45 JF-25-007 DMS-D6 2 1d_13C{1H} Charron - + - - - + +
48 13:58:56 JF-25-007 DMS-D6 1 1d_1H_Dsolv Charron + + - + + + +
50 13:15:24 WH-178-initial Br2 addition-Et2O 1 1d_1H_HSolv Chitnis + + - + + + + after addition of initial drops of Br2 and solution becomes clear
49 13:09:16 WH-178-pinacolone-Et2O 1 1d_1H_HSolv Chitnis + + - + + + + for monitoring
60 13:02:58 WH-178-bromopinacolone-CHCl3 1 1d_1H_HSolv Chitnis + + - + + + +
58 12:56:20 TJH-705-P2N2SP xtals Jan 28th 1 1d_31P{1H} Chitnis + - - + + + +
56 12:53:27 TOC03 2 1d_31P{1H} MacDonald - - - - - + + TOC03 31P{1H} unlock wide P(I) with NHC and S
56 12:47:02 TOC03 1 1d_31P{1H} MacDonald + + - + + + + TOC03 31P{1H} unlock P(I) with NHC and S
17 12:41:44 MAL-443-Aliqut-26h 2 1d_1H_HSolv Chitnis - + - - - + + Aliquot from scale up P2N4Me2(NTMS)2 in THF in quartz tube UVC 26h, very yellow soln
17 12:33:13 MAL-443-Aliqut-26h 1 1d_31P{1H} Chitnis + + - + + + + Aliquot from scale up P2N4Me2(NTMS)2 in THF in quartz tube UVC 26h, very yellow soln
55 12:17:12 KR012825-1 creatine formula peptide pH 2.5 1 1d_water Infusd + - - + + + +
54 12:01:08 KR012825-1 creatine original heated pH 2.5 1 1d_water Infusd + - - + + + +
53 11:44:55 KR012825-1 creatine original pH 2.5 1 1d_water Infusd + - - + + + +
28 11:39:34 MAL-446-10h 2 1d_1H_HSolv Chitnis - + - - - + + ALOT of P2N4Me2(NTMS)2 in EtOAc quartz tube UVC 10h, VERY pale yellow soln
28 11:31:12 MAL-446-10h 1 1d_31P{1H} Chitnis + + - + + + + ALOT of P2N4Me2(NTMS)2 in EtOAc quartz tube UVC 10h, VERY pale yellow soln
22 11:24:03 AP-25-001 1 1d_1H_Dsolv Charron + + - + + + +
59 11:20:43 RS (1)-13 Jan 28 T20 1 1d_31P{1H} Turculet + + - + + + +
43 11:14:02 Burke-x-83 1 1d_1H_Dsolv Speed + - - + + + +
42 11:07:07 Burke-x-82 1 1d_1H_Dsolv Speed + - - + + + +
41 11:00:43 Burke-x-81 1 1d_1H_Dsolv Speed + - - + + + +
52 10:50:15 KMEEEJ H NMR CDCL3 28.01.2025 400HZ 1 1d_1H_Dsolv Stradiotto + + - + + + + KMEEEJ H NMR CDCL3 28.01.2025 400HZ
59 10:44:49 RS (1)-13 Jan 28 T0 1 1d_31P{1H} Turculet + + - + + + +
29 10:36:24 JHB-52-A 2 1d_1H_Dsolv Thompson + - - + + + +
28 10:29:21 EBC-69-crude 1 1d_1H_Dsolv Thompson + + - + + + +
24 10:24:02 warren-vii-90 aliquot 400 11 1d_1H_HSolv Speed - + - - - + +
24 10:19:36 warren-vii-90 aliquot 400 10 1d_31P{1H} Speed + - - + + + +
22 09:51:11 TJH-718-P2N2 + P(NMe2)3 60 C overnight 1 1d_31P{1H} Chitnis + + - + + + +
20 09:44:01 MF208-4-33-6days-140C 2 1d_1H_HSolv Chitnis - + - - - + + 14days THF 80C- 6days dioxane 214 C
20 09:40:06 MF208-4-33-6days-140C 1 1d_31P{1H} Chitnis + + - + + + + 14days THF 80C- 6days dioxane 214 C
19 09:38:23 MF-P2-stability test-21days 3 1d_1H_Dsolv Chitnis - - - - - + +
19 09:37:23 MF-P2-stability test-21days 2 1d_31P{1H} Chitnis - - - - - + +
19 09:29:39 MF-P2-stability test-21days 1 1d_31P{1H} Chitnis + + - + + + +
51 08:56:44 KR012825 vitamin C formula 24H 1 1d_water Infusd + - - + + + +
40 23:28:32 KR012725 Vitamin C 10H 1 1d_water Infusd + + - + + + +
16 23:06:15 EO_635 3 2d_HSQC Jakeman - - - - - + + EO_635 biphenyl t1noisereduction: Noise region too small.
16 21:39:39 EO_635 2 1d_13C_UDEFT Jakeman + - - + + + + EO_635 biphenyl loopadj: Loop Filter = 124 Loop Gain = -1.36 Loop Time = 0.26
15 21:17:22 EO_634 4 2d_HSQC Jakeman - - - - - + + EO_634 fluoro t1noisereduction: Noise region too small.
15 19:50:49 EO_634 3 1d_13C_UDEFT Jakeman + - - + + + + EO_634 fluoro loopadj: Loop Filter = 115 Loop Gain = -1.92 Loop Time = 0.28
14 19:28:33 EO_633 3 2d_HSQC Jakeman - - - - - + + EO_633 t1noisereduction: Noise region too small.
14 18:00:22 EO_633 2 1d_13C_UDEFT Jakeman + + - + + + + EO_633 loopadj: Loop Filter = 111 Loop Gain = -2.20 Loop Time = 0.28
39 17:39:02 KR012725 Vitamin C 8H 1 1d_water Infusd + - - + + + +
38 17:23:13 KR012725 Vitamin C 6H 1 1d_water Infusd + - - + + + +
12 17:14:40 TJH-718-P2N2 + P(NMe2)3 1 1d_31P{1H} Chitnis + + - + + + +
6 16:40:15 1881-42-1 20 1d_1H_Dsolv SSPI + + - x - - - Lock failed after multiple attempts, lock: Command 'lock MeOD' failed. Lock is OFF, Command 'lock MeOD' failed. Lock is OFF
50 16:32:31 AN_046_H2O_27.01.2025 1 1d_1H_HSolv Chitnis + + - + + + + After work up ith DCM, Water layer
21 16:29:10 TJH-713-leftover soln Jan 27th 1 1d_31P{1H} Chitnis + - - + + + +
20 16:25:50 TJH-713-xtals Jan 27th 1 1d_31P{1H} Chitnis + - - + + + +
19 16:22:13 TJH-711-xtals Jan 27th 1 1d_31P{1H} Chitnis + - - + + + +
37 16:18:29 JT-chlorosilane aliquot 10 1d_31P{1H} Turculet + + - + + + +
11 16:13:23 warren-vii-90 aliquot 400 2 1d_1H_HSolv Speed - + - - - + +
11 16:08:24 warren-vii-90 aliquot 400 1 1d_31P{1H} Speed + + - + + + +
10 16:02:56 MAL-443-aliquot-16h 2 1d_1H_HSolv Chitnis - + - - - + + Aliquot from scale up P2N4Me2(NTMS)2 in THF in quartz tube UVC 16h total, very yellow soln. sat in gbox over weeked.
10 15:54:03 MAL-443-aliquot-16h 1 1d_31P{1H} Chitnis + + - + + + + Aliquot from scale up P2N4Me2(NTMS)2 in THF in quartz tube UVC 16h total, very yellow soln. sat in gbox over weeked.
5 15:38:30 1881-55-1 1 1d_1H_Dsolv SSPI + + - + + + +
4 15:27:30 1881-54-1 1 1d_1H_Dsolv SSPI + + - + + + +
33 15:10:43 KR012725 Vitamin C 4H 1 1d_water Infusd + + - + + + +
3 15:00:56 L1NY144006-38-3 1 1d_1H_Dsolv SSPI + - - + + + +
1 14:44:25 L1NY144007-1-1 1 1d_1H_Dsolv SSPI + + - + + + +
32 14:27:47 KR012725 Vitamin C 2H 1 1d_water Infusd + + - + + + +
30 14:20:12 JH-(1)-9-RngS2Second-H 1 1d_1H_Dsolv Turculet + - - + + + +
9 14:19:12 Burke-test box 3 23 1d_19F{1H} Speed - - - - - + + pp: Cannot find any peak for scaling in M:/data/Speed/nmr/Burke-test box 3/23/pdata/1/peaks!
9 14:12:26 Burke-test box 3 22 1d_1H_Dsolv Speed + - - + + + +
8 14:11:26 Burke-test box 2 13 1d_19F{1H} Speed - - - - - + + pp: Cannot find any peak for scaling in M:/data/Speed/nmr/Burke-test box 2/13/pdata/1/peaks!
8 14:03:53 Burke-test box 2 12 1d_1H_Dsolv Speed + - - + + + +
7 14:02:03 Burke-test box 1 2 1d_19F{1H} Speed - + - - - + +
7 13:54:31 Burke-test box 1 1 1d_1H_Dsolv Speed + + - + + + +
27 13:52:18 TOB114 42 1d_19F{1H} MacDonald - + - - - + + TOB114 19F{1H} unlock AN [LPPhF2]BF4 white crystal
27 13:49:43 TOB114 41 1d_31P{1H} MacDonald - + - - - + + TOB114 31P{1H} unlock AN [LPPhF2]BF4 white crystal pp: Cannot find any peak for scaling in M:/data/MacDonald/nmr/TOB114/41/pdata/1/peaks!
27 13:43:26 TOB114 40 1d_1H_HSolv MacDonald + + - + + + + TOB114 1H unlock AN [LPPhF2]BF4 white crystal
26 13:37:46 TOC02 1 1d_31P{1H} MacDonald + + - + + + + TOC02 31P{1H} unlock tol P(I) with NHC in DCM
25 13:34:41 TOC01 32 1d_31P{1H} MacDonald - - - - - + + TOC01 31P{1H} C6D6 P(I) with NHC, 1-octene, HSiEt3 overweekend
25 13:29:13 TOC01 31 1d_1H{31P} MacDonald - + - - - + + TOC01 1H{31P} C6D6 P(I) with NHC, 1-octene, HSiEt3 overweekend
25 13:21:01 TOC01 30 1d_1H_Dsolv MacDonald + + - + + + + TOC01 1H C6D6 P(I) with NHC, 1-octene, HSiEt3 overweekend
2 13:07:25 L1MA24035-70-1 1 1d_1H_Dsolv SSPI + + - + + + +
46 13:00:10 JHB-52-A 1 1d_1H_Dsolv Thompson + + - + + + +
45 12:57:23 PT-001-7d-Tol 1 1d_31P{1H} Chitnis + - - + + + +
20 12:52:23 TJH-717-P2N2 + P in hex 1 1d_31P{1H} Chitnis + + - + + + +
31 12:44:36 JH-(1)-9-RingS2-H 1 1d_1H_Dsolv Turculet + + - + + + +
16 12:38:55 EO_635 1 1d_1H_Dsolv Jakeman + - - + + + + EO_635 biphenyl
15 12:36:25 EO_634 2 1d_19F{1H} Jakeman - + - - - + + EO_634 fluoro
15 12:30:09 EO_634 1 1d_1H_Dsolv Jakeman + - - + + + + EO_634 fluoro
14 12:23:07 EO_633 1 1d_1H_Dsolv Jakeman + + - + + + + EO_633
18 12:17:52 DC-2025-002-27 2 1d_1H_HSolv Chitnis - + - - - + + NaH stoich Jan 27 (over wknd)
18 12:12:35 DC-2025-002-27 1 1d_31P{1H} Chitnis + - - + + + + NaH stoich Jan 27 (over wknd)
24 11:56:20 KR012725 creatine heated 96H 1 1d_water Infusd + - - + + + +
23 11:39:04 KR012725 creatine original 96H 1 1d_water Infusd + - - + + + +
49 11:22:32 KR012725 creatine our formula 96H 1 1d_water Infusd + - - + + + +
22 11:06:04 KR012725-1 Vit C formula 3 0H 1 1d_water Infusd + - - + + + +
55 11:01:20 JN-35-Toluene-Jan-27 2 1d_31P{1H} Chitnis - + - - - + + P2(NMe)4N(2-Pi) in Toluene Heated at 120C for 19 hrs Light green solution
55 10:54:17 JN-35-Toluene-Jan-27 1 1d_1H_HSolv Chitnis + + - + + + + P2(NMe)4N(2-Pi) in Toluene Heated at 120C for 19 hrs Light green solution
6 10:46:43 Burke-x-81 al2 1 1d_1H_Dsolv Speed + - - + + + +
53 10:37:55 AN_046_CDCl3 1 1d_1H_Dsolv Chitnis + + - + + + + 1 azido5 pentanol after extraction in DCM
5 10:35:22 Burke-x-80b 1 1d_19F{1H} Speed + - - + + + +
4 10:32:00 Burke-x-80a 10 1d_19F{1H} Speed + + - + + + +
3 10:29:51 Burke-x-84b 19 1d_31P{1H} Speed - + - - - + +
3 10:28:57 Burke-x-84b 18 1d_19F{1H} Speed - - - - - + +
3 10:26:53 Burke-x-84b 17 1d_19F{1H} Speed - + - - - + +
3 10:24:25 Burke-x-84b 16 1d_31P{1H} Speed - + - - - + +
3 10:17:54 Burke-x-84b 15 1d_1H_HSolv Speed + + - + + + +
2 10:15:45 Burke-x-84a 5 1d_31P{1H} Speed - + - - - + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, TopshimCheckLockAndSample - lock is off: please lock in prior to shimming FileHandlerTopSpin::chmod - : Unable to change permissions of file C:/Bruker/TopSpin4.1.4/data/topshimData: permissions: The system cannot find the file specified.: \"C:/Bruker/TopSpin4.1.4/data/topshimData\"
2 10:14:52 Burke-x-84a 4 1d_19F{1H} Speed - - - - - + +
2 10:12:51 Burke-x-84a 3 1d_19F{1H} Speed - + - - - + +
2 10:10:25 Burke-x-84a 2 1d_31P{1H} Speed - + - - - + +
2 10:04:10 Burke-x-84a 1 1d_1H_HSolv Speed + + - + + + +
1 09:56:43 Burke-x-83 al 1 1d_1H_Dsolv Speed + + - + + + +
7 19:59:16 JT-(3)-101 2 1d_31P{1H} Turculet - + - - - + +
7 19:52:17 JT-(3)-101 1 1d_1H_Dsolv Turculet + + - + + + +
48 17:09:54 3401-2025 Kyle C Exp 1 fraction 2 1 1d_1H_Dsolv DalChem + - - + + + +
47 17:03:02 3401-2025 Kyle C Exp 1 fraction 1 1 1d_1H_Dsolv DalChem + - - + + + +
46 16:56:07 3401-2025 Lauren A Exp 1 fraction 2 1 1d_1H_Dsolv DalChem + - - + + + +
45 16:49:19 3401-2025 Lauren A Exp 1 fraction 1 1 1d_1H_Dsolv DalChem + - - + + + +
44 16:42:37 3401-2025 Ethan B Exp 1 fraction 2 1 1d_1H_Dsolv DalChem + - - + + + +
43 16:35:21 3401-2025 Ethan B Exp 1 fraction 1 1 1d_1H_Dsolv DalChem + - - + + + +
42 16:30:02 3401-2025 Brendan S Exp 3 2 1d_13C{1H} DalChem - - - - - + + 2-chlorotoluene
42 16:22:57 3401-2025 Brendan S Exp 3 1 1d_1H_Dsolv DalChem + - - + + + + 2-chlorotoluene
41 16:17:40 3401-2025 Jane C Expt 2 Day 2 2 1d_13C{1H} DalChem - - - - - + +
41 16:11:06 3401-2025 Jane CExpt 2 Day 2 1 1d_1H_Dsolv DalChem + - - + + + +
40 16:05:48 3401-2025 Ella M Expt 2 Day 2 2 1d_13C{1H} DalChem - - - - - + +
40 15:58:43 3401-2025 Ella M Expt 2 Day 2 1 1d_1H_Dsolv DalChem + - - + + + +
6 11:27:17 CHEM 3401 Reece O'Brien Exp. 3 4 1d_13C{1H} DalChem - - - - - + +
6 11:20:42 CHEM 3401 Reece O'Brien Exp. 3 3 1d_1H_Dsolv DalChem + - - + + + +
5 11:15:25 CHEM 3401 Damian M. A. Exp. 3 2 1d_13C{1H} DalChem - - - - - + +
5 11:09:12 CHEM 3401 Damian M. A. Exp. 3 1 1d_1H_Dsolv DalChem + - - + + + +
4 11:02:27 CHEM 3401 Alex Petkov Exp. 3 2 1d_13C{1H} DalChem - + - - - + +
4 10:55:41 CHEM 3401 Alex Petkov Exp. 3 1 1d_1H_Dsolv DalChem + - - + + + +
3 10:49:15 CHEM 3401 Hafsa Kuccukoglu Exp. 2 Day 1 1 1d_1H_Dsolv DalChem + - - + + + +
2 10:42:19 CHEM 3401 Katie Cox Exp. 2 Day 1 1 1d_1H_Dsolv DalChem + - - + + + +
1 10:34:52 CHEM 3401 Jane Courtney Exp. 2 Day 1 1 1d_1H_Dsolv DalChem + + - + + + +
21 15:14:58 burke-x-84a-Jan25 5 1d_31P{1H} Speed - - - - - + +
21 15:12:25 burke-x-84a-Jan25 4 1d_31P{1H} Speed - + - - - + +
21 15:11:32 burke-x-84a-Jan25 3 1d_19F{1H} Speed - - - - - + +
21 15:08:43 burke-x-84a-Jan25 2 1d_19F{1H} Speed - + - - - + +
21 15:02:21 burke-x-84a-Jan25 1 1d_1H_HSolv Speed + + - + + + +
20 20:21:54 BM_Rxn3b_peak1_CDCl3 1 1d_1H_Dsolv Baker + - - + + + +
19 20:15:12 EBC-68-benzaldehyde 1 1d_1H_Dsolv Thompson + - - + + + +
18 20:08:45 EBC-68-propiophenone 1 1d_1H_Dsolv Thompson + - - + + + +
17 20:01:35 EBC-68-crude 1 1d_1H_Dsolv Thompson + + - + + + +
39 19:51:18 1402-23-5 1 1d_1H_Dsolv SSPI + + - + + + +
38 19:31:55 L1CA42013-28-1 1 1d_1H_Dsolv SSPI + + - + + + +
37 19:24:41 L1CA42013-27-1 1 1d_1H_Dsolv SSPI + - - + + + +
36 19:14:46 L1CA42013-17-9 1 1d_1H_Dsolv SSPI + - - + + + +
35 19:04:57 L1CA42013-17-7 1 1d_1H_Dsolv SSPI + - - + + + +
34 18:54:53 L1CA42013-13-17 1 1d_1H_Dsolv SSPI + - - + + + +
33 18:44:57 L1CA42013-13-15 1 1d_1H_Dsolv SSPI + - - + + + +
32 18:37:35 L1CA187001-76-1 1 1d_1H_Dsolv SSPI + - - + + + +
31 18:30:16 L1CA187001-73-1 1 1d_1H_Dsolv SSPI + - - + + + +
30 18:13:58 L1MA105005-44-1-2 1 1d_1H_Dsolv SSPI + + - + + + +
16 17:58:03 EXP-294 DEPT 6 1d_13C_DEPT Bearne - - - - - + +
16 17:37:52 EXP-294 13C 5 1d_13C{1H} Bearne - - - - - + +
16 17:30:24 EXP-294 1H 4 1d_1H_Dsolv Bearne + - - + + + +
15 17:22:07 2025-01-24 - Substrate for NSAR DEPT 6 1d_13C_DEPT Bearne - - - - - + + pp: Unable to assign a peak for scaling of M:/data/Bearne/nmr/2025-01-24 - Substrate for NSAR DEPT/6/pdata/1/peaks No peak is found in the specified ranges!
15 17:11:17 2025-01-24 - Substrate for NSAR 13C 5 1d_13C{1H} Bearne - + - - - + + pp: Unable to assign a peak for scaling of M:/data/Bearne/nmr/2025-01-24 - Substrate for NSAR 13C/5/pdata/1/peaks No peak is found in the specified ranges!
15 17:03:54 2025-01-24 - Substrate for NSAR 1H 4 1d_1H_Dsolv Bearne + + - + + + +
13 16:58:25 MAL-445-4h 2 1d_1H_HSolv Chitnis - + - - - + + P2N4Me2(NTMS)2 in 2,3-dimethyl-1,3-butadiene in quartz tube UVC ~4hr, cc soln with white semi-xtalline ppt
13 16:49:51 MAL-445-4h 1 1d_31P{1H} Chitnis + + - + + + + P2N4Me2(NTMS)2 in 2,3-dimethyl-1,3-butadiene in quartz tube UVC ~4hr, cc soln with white semi-xtalline ppt
12 16:45:10 Muise-ii-33-al 2 1d_31P{1H} Speed - + - - - + +
12 16:37:39 Muise-ii-33-al 1 1d_1H_Dsolv Speed + + - + + + +
29 16:25:26 1881-51-1 1 1d_1H_Dsolv SSPI + + - + + + +
53 16:15:28 AN_046_H2O_24.01.2025 1 1d_1H_HSolv Chitnis + + - + + + + 5 aminopentanol to 1 azido 5pentanol
11 16:11:15 MAL-440-Aliquot-2d-105C 3 1d_1H_HSolv Chitnis - + - - - + + Aliquot from PCl3 + Et3N + cyN2.2HCl in toluene 90C 1d then 105C 2 day yellow soln
11 16:06:00 MAL-440-Aliquot-2d-105C 2 1d_1H_HSolv Chitnis - + - - - + + Aliquot from PCl3 + Et3N + cyN2.2HCl in toluene 90C 1d then 105C 2 day yellow soln
11 15:57:41 MAL-440-Aliquot-2d-105C 1 1d_31P{1H} Chitnis + + - + + + + Aliquot from PCl3 + Et3N + cyN2.2HCl in toluene 90C 1d then 105C 2 day yellow soln
28 15:49:49 1881-53-1 1 1d_1H_Dsolv SSPI + + - + + + +
47 15:47:32 MM-72.3-10 SbCl3 + P2N6 1 day THF rt 2 1d_31P{1H} Chitnis - + - - - + +
47 15:43:18 MM-72.3-10 SbCl3 + P2N6 1 day THF rt 1 1d_1H_Dsolv Chitnis + + - + + + +
45 15:40:14 TOC01 22 1d_31P{1H} MacDonald - - - - - + + TOC01 31P{1H} C6D6 P(I) with NHC, 1-octene, Et3iH
45 15:34:09 TOC01 21 1d_1H{31P} MacDonald - + - - - + + TOC01 1H{31P} C6D6 P(I) with NHC, 1-octene, Et3iH
45 15:26:39 TOC01 20 1d_1H_Dsolv MacDonald + + - + + + + TOC01 1H C6D6 P(I) with NHC, 1-octene, Et3iH
44 15:21:22 TJH-715-P2N2 + Bi in thf 2 1d_1H_HSolv Chitnis - + - - - + +
44 15:17:23 TJH-715-P2N2 + Bi in thf 1 1d_31P{1H} Chitnis + + - + + + +
43 15:10:47 kca-3 3 1 1d_1H_Dsolv Thompson + - - + + + +
42 15:04:16 kca-3 2 1 1d_1H_Dsolv Thompson + - - + + + +
41 14:57:07 kca-3 1 1 1d_1H_Dsolv Thompson + + - + + + +
40 14:53:23 PT-001-4d-Tol 1 1d_31P{1H} Chitnis + + - + + + +
27 14:47:24 1881-52-1 1 1d_1H_Dsolv SSPI + - - + + + +
26 14:39:54 1881-50-1 1 1d_1H_Dsolv SSPI + - - + + + +
25 14:32:27 1881-49-1 1 1d_1H_Dsolv SSPI + - - + + + +
24 14:25:09 1881-48-1 1 1d_1H_Dsolv SSPI + - - + + + +
23 14:17:53 1881-45-1 1 1d_1H_Dsolv SSPI + - - + + + +
22 14:10:04 1881-42-1 10 1d_1H_Dsolv SSPI + + - + + + +
20 13:40:31 AP-24-Nahpthoxz 1 1d_1H_Dsolv Charron + + - + + + +
56 13:24:46 Pt-002-2nd 1 1d_31P{1H} Chitnis + + - + + + +
34 13:19:42 MAL-445-1h 2 1d_1H_HSolv Chitnis - + - - - + + P2N4Me2(NTMS)2 in 2,3-dimethyl-1,3-butadiene in quartz tube UVC 1h cc sln some white solids
34 13:11:03 MAL-445-1h 1 1d_31P{1H} Chitnis + + - + + + + P2N4Me2(NTMS)2 in 2,3-dimethyl-1,3-butadiene in quartz tube UVC 1h cc sln some white solids