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IconNMR Automation Run Status:
Day Experiments: 00:00
Busy Until: Thu 12:34
Night Experiments: 02:09

Setup List
Holder Status Name ExpNo Experiment User Time Title
2 Submitted aa83-2Na-d2o 4 N 1d_13C_UDEFT 13C UDEFT Experiment Jakeman 01:38:49
2 Submitted aa83-2Na-d2o 5 N 2d_HSQC Standard 1H-13C HSQC Experiment Jakeman 00:10:53
2 Submitted aa83-2Na-d2o 6 N 2d_HMBC Standard 1H-13C HMBC Experiment Jakeman 00:19:36
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
28 12:25:30 JF-25-093 Crude 2 1d_13C{1H} Charron - + - - - + +
28 12:18:27 JF-25-093 Crude 1 1d_1H_Smart Charron + + - + + + +
2 10:26:45 aa83-2Na-d2o 3 1d_19F{1H} Jakeman - + - - - + +
2 10:25:42 aa83-2Na-d2o 2 1d_31P{1H} Jakeman - - - - - + +
2 10:16:03 aa83-2Na-d2o 1 1d_1H_Smart Jakeman + + - + + + +
29 09:35:17 TOD33 1 1d_31P{1H} MacDonald + + - + + + + TOD33 31P{1H} unlock in THF/Et2O Crude
2 09:31:35 aa97-80C-24h 2 1d_19F{1H} Jakeman - + - - - + +
2 09:26:21 aa97-80C-24h 1 1d_31P{1H} Jakeman + + - + + + + topshim: Diverging behaviour detected during shimming.
23 09:19:01 MFA38-3 1 1d_1H_Smart Thompson + + - + + + + after column-3
22 09:11:47 MFA38-2 1 1d_1H_Smart Thompson + + - + + + + after column, 2 and mainly 3
21 09:04:40 MFA38-1 1 1d_1H_Smart Thompson + + - + + + + after column-mix 2 and 3
19 17:34:47 L1SSPI043-35-1_Cyclone 1 1d_1H_Smart SSPI + + - + + + +
18 17:27:19 L1SSPI042-36-1_Collection 1 1d_1H_Smart SSPI + + - + + + +
17 17:19:41 L1SSPI042-34-1_Collection 1 1d_1H_Smart SSPI + + - + + + +
16 17:12:03 L1SSPI042-32-1_Bottom 1 1d_1H_Smart SSPI + + - + + + +
15 17:04:31 L1MA24033-107-5 1 1d_1H_Smart SSPI + + - + + + +
14 16:48:59 L1MA24033-107-1 1 1d_1H_Smart SSPI + + - + + + +
13 16:41:20 L1MA24033-93-17 1 1d_1H_Smart SSPI + + - + + + +
12 16:33:26 L1MA24033-93-7 1 1d_1H_Smart SSPI + + - + + + +
11 16:25:58 L1MA24033-101-6_air dry 1 1d_1H_Smart SSPI + + - + + + +
10 16:18:14 L1MA24033-102-1 1 1d_1H_Smart SSPI + + - + + + +
9 16:10:30 L1MA24033-92-20 1 1d_1H_Smart SSPI + + - + + + +
8 16:02:49 L1MA24033-90-7 1 1d_1H_Smart SSPI + + - + + + +
7 15:55:09 L1MA24033-90-4 1 1d_1H_Smart SSPI + + - + + + +
6 15:47:30 L1MA24033-90-1 1 1d_1H_Smart SSPI + + - + + + +
5 15:31:48 L1BC166014-13-1 1 1d_1H_Smart SSPI + + - + + + +
4 15:15:47 L1BC166014-20-3 1 1d_1H_Smart SSPI + + - + + + +
20 15:08:13 EHA-48 1 1d_1H_Smart Thompson + + - + + + +
3 14:58:08 1057-74-1 1 1d_1H_Smart SSPI + + - + + + +
1 13:42:00 Dextran-Nb with 0.25 Eq. in DMSO after lyophilization 1 1d_1H_Smart Baker + + - + + + + Dextran-Nb with 0.25 Eq. in DMSO after lyophilization
36 11:08:56 TAG 27 30 1d_31P{1H} MacDonald + - - + + + + TAG 27, 1 drop P(NMe2)3 added 31P{1H}, CH3CN, 2025-09-03
30 10:54:55 JN-86.1-P2N4Cl2-Toluene-100C-24hrs-Sept-3 1 1d_31P{1H} Chitnis + + - + + + + P2N4Cl2 in toluene Heated at 100C for 24 hrs light yello soln
27 10:40:20 JN-86-P2N4Cl2-100C-24hrs-Toluene-Sept-3 1 1d_31P{1H} Chitnis + x - - - - - P2N4Cl2 ring in toluene heated at 100C for 24 hrs light yellow solution log_err: Important data in the probe memory is erroneous. Details:, ATM Failed
1 09:25:00 aa97 10 1d_19F{1H} Reservation + + - + + + +
1 09:20:01 aa97 9 1d_31P{1H} Reservation + + - + + + +
1 03:25:01 aa97 8 1d_19F{1H} Reservation + + - + + + +
1 03:20:01 aa97 7 1d_31P{1H} Reservation + + - + + + +
1 21:25:00 aa97 6 1d_19F{1H} Reservation + + - + + + +
1 21:20:00 aa97 5 1d_31P{1H} Reservation + - - + + + +
59 17:05:21 PP or Monteal F1 1 1d_1H{31P} Adibnia + - - + + + +
60 16:35:48 PP for Montreal f1 of F1 1 1d_1H{31P} Adibnia + + - + + + +
1 15:25:01 aa97 4 1d_19F{1H} Reservation + + - + + + +
1 15:20:00 aa97 3 1d_31P{1H} Reservation + - - + + + +
36 15:04:23 TAG 27 12 1d_31P{1H} MacDonald + - - + + + + TAG 27, PCl3 31P{1H}, CH3CN, 2025-09-02
35 14:56:45 TAG 27 3 1d_31P{1H} MacDonald + - - + + + + TAG 27 31P{1H}, CH3CN, 2025-09-02
37 14:50:56 TAG 27 22 1d_31P{1H} MacDonald - - - - - + + TAG 27, P(NMe2)3 31P{1H}, CH3CN, 2025-09-02
37 14:49:55 TAG 27 21 1d_31P{1H} MacDonald - - - - - + + TAG 27, P(NMe2)3 31P{1H}, CH3CN, 2025-09-02
37 14:44:13 TAG 27 20 1d_1H_Smart MacDonald + + - + + + + TAG 27, P(NMe2)3 1H, CH3CN, 2025-09-02
36 14:43:10 TAG 27 11 1d_31P{1H} MacDonald - - - - - + + TAG 27, PCl3 31P{1H}, CH3CN, 2025-09-02
36 14:37:18 TAG 27 10 1d_1H_Smart MacDonald + + - + + + + TAG 27, PCl3 1H, CH3CN, 2025-09-02
35 14:34:43 TAG 27 2 1d_31P{1H} MacDonald - + - - - + + TAG 27 31P{1H}, CH3CN, 2025-09-02
35 14:28:15 TAG 27 1 1d_1H_Smart MacDonald + + - + + + + TAG 27 1H, CH3CN, 2025-09-02
1 12:29:57 aa97 2 1d_19F{1H} Reservation - + - - - + +
1 12:26:04 aa97 1 1d_31P{1H} Reservation + - - + + + +
39 11:59:42 TOD32 1 1d_31P{1H} MacDonald + - - + + + + TOD32 31P{1H} unlock in Tol P(I) with PS(NMe2)3
37 11:34:35 Reagent Check 10 1d_1H_Smart MacDonald + + - + + + + Benzyl BZIMPY 1H, CH3CN, 2025-09-02 topshim: Diverging behaviour detected during shimming.
36 11:32:14 Ksenia Samples 43 1d_31P{1H} MacDonald - + - - - + + KF 13C 31P{1H}, CH2Cl2, 2025-09-02
36 11:27:55 Ksenia Samples 42 1d_19F{1H} MacDonald - + - - - + + KF 13C 19F{1H}, CH2Cl2, 2025-09-02
36 11:24:24 Ksenia Samples 41 1d_11B{1H} MacDonald - + - - - + + KF 13C 11B{1H}, CH2Cl2, 2025-09-02
36 11:18:56 Ksenia Samples 40 1d_1H_Smart MacDonald + + - + + + + KF 13C 1H, CH2Cl2, 2025-09-02
35 11:16:23 Ksenia Samples 33 1d_31P{1H} MacDonald - + - - - + + KF 10 31P{1H}, CH3CN, 2025-09-02
35 11:14:02 Ksenia Samples 32 1d_19F{1H} MacDonald - + - - - + + KF 10 19F{1H}, CH3CN, 2025-09-02
35 11:07:30 Ksenia Samples 30 1d_1H_Smart MacDonald + + - + + + + KF 10 1H, CH3CN, 2025-09-02
17 10:43:10 JF-25-091 Purified 2 1d_13C{1H} Charron - - - - - + +
17 10:35:53 JF-25-091 Purified 1 1d_1H_Smart Charron + + - + + + +
16 10:28:52 JF-25-089 Purified 2 1d_13C{1H} Charron - + - - - + +
16 10:21:46 JF-25-089 Purified 1 1d_1H_Smart Charron + + - + + + +
15 09:19:24 TOD31 10 1d_31P{1H} MacDonald + + - + + + + TOD31 31P{H} unlock in tol PS(NMe2)3
14 18:22:39 Inulin-Nb (2nd functionalization in DMSO) 1 1d_1H_Smart Baker + + - + + + + Inulin-Nb in DMSO (2nd functioanaization)
13 17:53:18 Inulin-Nb (after adding more Nb in 2nd Functionalization) 1 1d_1H_Smart Baker + + - + + + + Inulin-Nb 2nd Functionalization
12 17:24:05 Inulin-COOH new method 1 1d_1H_Smart Baker + + - + + + + Inulin-COOH new method
11 16:54:51 BCD-COOH -method 1 1d_1H_Smart Baker + + - + + + + BCD-COOH
10 16:25:32 BCD-pure 1 1d_1H_Smart Baker + + - + + + + BCD pur
9 16:19:22 WH-227-MeAsH-THF protio-15 min 1 1d_1H_Smart Chitnis + + - + + + + lithiation route. went from plae pnk ligand to yellow lithiated. then to red orange after AsCl3
52 15:33:56 TOD31 1 1d_31P{1H} MacDonald + - - + + + + TOD31 31P{1H} unlock in Tol P(NMe2)3
51 14:35:00 PT-087-2d100-P4+PheolAz-Dioxane 2 1d_31P{1H} Chitnis + - - + + + + lots of orange ppt, the solution in the tube is not clear
51 14:16:25 PT-087-2d100-P4+PheolAz-Dioxane 1 1d_31P{1H} Chitnis + - - + + + + lots of orange ppt, the solution in the tube is not clear
58 22:37:00 PT-077_1-Py 2 1d_31P{1H} Chitnis + + - + + + + clean yellow solution
19 22:16:20 aa79-Na-meod4 7 2d_HMBC Jakeman - - - - - + +
19 22:04:27 aa79-Na-meod4 6 2d_HSQC Jakeman - - - - - + +
19 20:19:52 aa79-Na-meod4 5 1d_13C_UDEFT Jakeman + + - + + + + loopadj: Loop Filter = 101 Loop Gain = -2.95 Loop Time = 0.30
17 19:59:20 aa72-Na-d2o 6 2d_HMBC Jakeman - - - - - + +
17 19:47:34 aa72-Na-d2o 5 2d_HSQC Jakeman - - - - - + + pp: Unable to assign a peak for scaling of M:/data/Jakeman/nmr/aa72-Na-d2o/5/pdata/9999/peaks No peak is found in the specified ranges!; t1noisereduction: SAXParseException: unable to open primary document entity 'M:/data/Jakeman/nmr/aa72-Na-d2o/5/pdata/9999/peaklist.xml', no peak found
17 18:00:11 aa72-Na-d2o 4 1d_13C_UDEFT Jakeman + + - + + + + loopadj: Loop Filter = 136 Loop Gain = -0.62 Loop Time = 0.25
36 16:17:00 TAG 20 11 1d_31P{1H} MacDonald - - - - - + + TAG 20, Isolated final solid 31P{1H}, CDCl3, 2025-08-28
36 16:05:15 TAG 20 10 1d_1H_Smart MacDonald + + - + + + + TAG 20, Isolated final solid 1H, CDCl3, 2025-08-28
20 16:02:24 TOD30 22 1d_31P{1H} MacDonald - - - - - + + TOD30 31P unlock in THF P(I) with 13 eq Ph(OH)2
20 15:58:04 TOD30 21 1d_31P{1H} MacDonald - + - - - + + TOD30 31P{1H} unlock in THF P(I) with 13 eq Ph(OH)2
20 15:51:40 TOD30 20 1d_1H_Smart MacDonald + + - + + + + TOD30 1H unlock in THF P(I) with 13 eq Ph(OH)2
19 15:49:12 aa79-Na-meod4 4 1d_19F{1H} Jakeman - + - - - + +
19 15:46:40 aa79-Na-meod4 3 1d_31P{1H} Jakeman - + - - - + +
19 15:37:45 aa79-Na-meod4 1 1d_1H_Smart Jakeman + + - + + + +
18 15:35:01 aa96 4 1d_19F{1H} Reservation + + - + + + +
18 15:30:01 aa96 3 1d_31P{1H} Reservation + + - + + + +
6 13:57:11 TOD26 21 1d_31P{1H} MacDonald - - - - - + + TOD26 31P{1H} in CDCl3 P(PhBr)3 3rd
6 13:50:17 TOD26 20 1d_1H_Smart MacDonald + + - + + + + TOD26 1H in CDCl3 P(PhBr)3 3rd
3 13:38:21 AN_163(2crystal)_CDCl3_28.08.2025 2 1d_31P{1H} Chitnis - - - - - + +
3 13:30:55 AN_163(2crystal)_CDCl3_28.08.2025 1 1d_1H_Smart Chitnis + + - + + + +
2 13:29:53 AN_163_(1crystal)_CDCl3_28.08.2025 2 1d_31P{1H} Chitnis - - - - - + +
2 13:22:48 AN_163_(1crystal)_CDCl3_28.08.2025 1 1d_1H_Smart Chitnis + + - + + + +
24 12:55:23 AN_163_crstal2_28.08.2025 2 1d_31P{1H} Chitnis - + - - - + + AN_163_Crystal1(big)_DMSO_28.08.2025
24 12:48:46 AN_163_crstal2_28.08.2025 1 1d_1H_Smart Chitnis + + - + + + + AN_163_Crystal1(big)_DMSO_28.08.2025
18 12:45:10 aa96 2 1d_19F{1H} Reservation + + - + + + +
23 12:44:08 AN_163_Crystal1_DMSO_28.08.2025 2 1d_31P{1H} Chitnis - - - - - + + AN_163 crystal 1small_in dmso_
23 12:38:07 AN_163_Crystal1_DMSO_28.08.2025 1 1d_1H_Smart Chitnis + + - + + + + AN_163 crystal 1small_in dmso_
18 12:33:20 aa96 1 1d_31P{1H} Reservation + - - + + + +
22 12:32:13 AN_159_28.08.2025_DMSO 2 1d_31P{1H} Chitnis - - - - - + + AN_159 _PPt in pentane_not crystallized_washed with Et2O_in DMSO(not dueterated)
22 12:26:26 AN_159_28.08.2025_DMSO 1 1d_1H_Smart Chitnis + + - + + + + AN_159 _PPt in pentane_not crystallized_washed with Et2O_in DMSO(not dueterated)
19 10:49:56 TOD30 12 1d_31P{1H} MacDonald - - - - - + + TOD30 31P unlock in THF P(I) with Ph(OH)2 pp: Cannot find any peak for scaling in M:/data/MacDonald/nmr/TOD30/12/pdata/1/peaks!
19 10:45:30 TOD30 11 1d_31P{1H} MacDonald - + - - - + + TOD30 31P{1H} unlock in THF P(I) with Ph(OH)2 pp: Cannot find any peak for scaling in M:/data/MacDonald/nmr/TOD30/11/pdata/1/peaks!
19 10:39:10 TOD30 10 1d_1H_Smart MacDonald + + - + + + + TOD30 1H unlock in THF P(I) with Ph(OH)2
17 10:36:44 aa72-Na-d2o 3 1d_19F{1H} Jakeman - + - - - + +
17 10:34:01 aa72-Na-d2o 2 1d_31P{1H} Jakeman - + - - - + +
17 10:25:05 aa72-Na-d2o 1 1d_1H_Smart Jakeman + + - + + + +
16 10:01:55 TOD26 12 1d_13C{1H} MacDonald - + - - - + + TOD26 13C{1H} in CDCl3 P(PhBr)3
16 09:57:36 TOD26 11 1d_31P{1H} MacDonald - + - - - + + TOD26 31P{1H} in CDCl3 P(PhBr)3
16 09:50:30 TOD26 10 1d_1H_Smart MacDonald + + - + + + + TOD26 1H in CDCl3 P(PhBr)3
13 19:42:04 aa77-Na-meod4 6 2d_HMBC Jakeman - - - - - + +
13 19:30:18 aa77-Na-meod4 5 2d_HSQC Jakeman - - - - - + +
13 18:00:06 aa77-Na-meod4 4 1d_13C_UDEFT Jakeman + + - + + + + loopadj: Loop Filter = 110 Loop Gain = -2.29 Loop Time = 0.29
33 16:22:44 L1SSPI042-32-1 1 1d_1H_Smart SSPI + + - + + + +
43 16:19:41 TAG 22 15 1d_31P{1H} MacDonald - - - - - + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 31P{1H}, CH3CN, 2025-08-27
43 16:13:47 TAG 22 14 1d_31P{1H} MacDonald + + - + + + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 31P{1H}, CH3CN, 2025-08-27 pp: Cannot find any peak for scaling in M:/data/MacDonald/nmr/TAG 22/14/pdata/1/peaks!
32 16:06:02 L1SSPI038-36-1 1 1d_1H_Smart SSPI + + - + + + +
31 15:58:03 L1SSPI042-28-1 1 1d_1H_Smart SSPI + + - + + + +
46 15:54:19 TAG 18 13 1d_11B{1H} MacDonald - + - - - + + TAG 18, [BnBZIMPY PPh][BArF24]2, Filtrate dried 11B{1H}, CH2Cl2, 2025-08-27
46 15:51:56 TAG 18 12 1d_19F{1H} MacDonald - + - - - + + TAG 18, [BnBZIMPY PPh][BArF24]2, Filtrate dried 19F{1H}, CH2Cl2, 2025-08-27
46 15:50:56 TAG 18 11 1d_31P{1H} MacDonald - - - - - + + TAG 18, [BnBZIMPY PPh][BArF24]2, Filtrate dried 31P{1H}, CH2Cl2, 2025-08-27
46 15:45:18 TAG 18 10 1d_1H_Smart MacDonald + + - + + + + TAG 18, [BnBZIMPY PPh][BArF24]2, Filtrate dried 1H, CH2Cl2, 2025-08-27
45 15:44:16 PPh3 2 1d_31P{1H} MacDonald - - - - - + + PPh3 31P{1H}, CH3CN, 2025-08-27
45 15:38:28 PPh3 1 1d_1H_Smart MacDonald + + - + + + + PPh3 1H, CH3CN, 2025-08-27
44 15:36:01 Tetraphenyl Phosphonium Chloride 2 1d_31P{1H} MacDonald - + - - - + + [PPh4][Cl] 31P{1H}, CH3CN, 2025-08-27
44 15:30:09 Tetraphenyl Phosphonium Chloride 1 1d_1H_Smart MacDonald + + - + + + + [PPh4][Cl] 1H, CH3CN, 2025-08-27
43 15:26:57 TAG 22 13 1d_7Li MacDonald - + - - - + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 7Li, CH3CN, 2025-08-27 pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of M:/data/MacDonald/nmr/TAG 22/13/pdata/1/peaks!
43 15:23:28 TAG 22 12 1d_11B{1H} MacDonald - + - - - + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 11B{1H}, CH3CN, 2025-08-27
43 15:22:27 TAG 22 11 1d_31P{1H} MacDonald - - - - - + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 31P{1H}, CH3CN, 2025-08-27 pp: Cannot find any peak for scaling in M:/data/MacDonald/nmr/TAG 22/11/pdata/1/peaks!
43 15:15:32 TAG 22 10 1d_1H_Smart MacDonald + + - + + + + TAG 22 AllylZIMPY SbCl3 + PPh3 en LiBH4 2.8 mg 1H, CH3CN, 2025-08-27
30 15:07:51 L1A22067-28-1 1 1d_1H_Smart SSPI + + - + + + +
29 14:57:41 L1BC166013-8-4 1 1d_1H_Smart SSPI + + - + + + +
28 14:47:16 L1BC166013-4-10 1 1d_1H_Smart SSPI + + - + + + +
27 14:36:47 L1BC166013-3-11 1 1d_1H_Smart SSPI + + - + + + +
56 14:06:15 PT-087-1d70-P4+Phenol-Diox 2 1d_31P{1H} Chitnis + + - + + + + brown solution not clear
14 14:03:52 aa86-80C-24h 2 1d_19F{1H} Jakeman - + - - - + +
14 13:57:40 aa86-80C-24h 1 1d_31P{1H} Jakeman + + - + + + +
13 13:55:27 aa77-Na-meod4 3 1d_19F{1H} Jakeman - + - - - + +
13 13:54:25 aa77-Na-meod4 2 1d_31P{1H} Jakeman - - - - - + +
13 13:45:09 aa77-Na-meod4 1 1d_1H_Smart Jakeman + + - + + + +
34 12:15:43 TAG 22 2 1d_31P{1H} MacDonald - - - - - + + TAG 22, AllylBZIMPY-SbCl3 + PPh3 31P{1H}, CH3CN, 2025-08-27
34 12:09:20 TAG 22 1 1d_1H_Smart MacDonald + + - + + + + TAG 22, AllylBZIMPY-SbCl3 + PPh3 1H, CH3CN, 2025-08-27
33 12:06:17 TAG 20 2 1d_31P{1H} MacDonald - - - - - + + TAG 20, AllylBZIMPY-SbCl3 + [PPh4][Cl] 31P{1H}, CH3CN, 2025-08-27
33 11:59:49 TAG 20 1 1d_1H_Smart MacDonald + + - + + + + TAG 20, AllylBZIMPY-SbCl3 + [PPh4][Cl] 31P{1H}, CH3C, 2025-08-27
54 11:39:28 PT-087-1d70-P4+Phenol-Doix 1 1d_31P{1H} Chitnis + - - + + + + brown solution, not clear
53 11:34:56 PT-077_1-Py 1 1d_31P{1H} Chitnis + + - + + + + solid ppt from the P4+BAAz reaction dissolved in Py - orange solution
5 11:12:25 AN_148_(1)_CDCl3 2 1d_31P{1H} Chitnis - - - - - + +
5 11:05:45 AN_148_(1)_CDCl3 1 1d_1H_Smart Chitnis + + - + + + + AN148 in CDCL3
3 10:45:13 AN_48_27.08.2025 2 1d_31P{1H} Chitnis - - - - - + + pp: Cannot find any peak for scaling in M:/data/Chitnis/nmr/AN_48_27.08.2025/2/pdata/1/peaks!
3 10:38:14 AN_48_27.08.2025 1 1d_1H_Smart Chitnis + + - + + + +
2 10:15:43 AN_PNBPA_27.08.2025_THF 2 1d_31P{1H} Chitnis - + - - - + +
2 10:10:07 AN_PNBPA_27.08.2025_THF 1 1d_1H_Smart Chitnis + + - + + + + PNBP reaction overnight