Setup List
| Holder |
Status |
Name |
ExpNo |
Experiment |
User |
Time |
Title |
| 1 |
Completed |
Burke-xii-35 al2 |
1 |
N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) |
Speed |
00:01:24 |
|
| 2 |
Completed |
Burke-xii-30b hex |
1 |
N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) |
Speed |
00:01:30 |
|
| 3 |
Completed |
Burke-xii-32 dmso |
1 |
N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) |
Speed |
00:01:24 |
|
| 5 |
Completed |
L1GA188001-79-1-b_MeOD |
1 |
N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) |
SSPI |
00:10:53 |
|
| 6 |
Completed |
L1GA188001-1-1-b_MeOD |
1 |
N 1d_1H_Dsolv Standard 1D Proton (For Samples in Deuterated Solvent) |
SSPI |
00:10:53 |
|
| 9 |
Completed |
MAL-NacNacP-xtals |
1 |
N 1d_31P{1H} 31P Observe with 1H Decoupling |
MacDonald |
00:17:13 |
NacNacP-Na-THF supernate - orange solution THF / pentane, crystals grew in this, but brown NaPH2 goo at bottom removed |
| 9 |
Completed |
MAL-NacNacP-xtals |
2 |
N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) |
MacDonald |
00:01:24 |
NacNacP-Na-THF supernate - orange solution THF / pentane, crystals grew in this, but brown NaPH2 goo at bottom removed |
| 54 |
Completed |
PT-083_2-air_3d-Dioxane |
1 |
N 1d_31P{1H} 31P Observe with 1H Decoupling |
Chitnis |
00:11:05 |
clear colourless (the vial is foggy) |
| 55 |
Completed |
PT-077_2-after1wash-Dioxane |
1 |
N 1d_31P{1H} 31P Observe with 1H Decoupling |
Chitnis |
00:22:00 |
colourless cloudy |
| 55 |
Completed |
PT-077_2-after1wash-Dioxane |
2 |
N 1d_1H_HSolv 1D Proton with Solvent Peak Removal (Samples in Protio Solvent) |
Chitnis |
00:15:28 |
colourless cloudy |
| 55 |
Completed |
PT-077_2-after1wash-Dioxane |
3 |
N 1d_13C{1H} 13C Observe with 1H Decoupling |
Chitnis |
01:39:21 |
colourless cloudy |
| 55 |
Completed |
PT-077_2-after1wash-Dioxane |
4 |
N 1d_13C_UDEFT 13C UDEFT Experiment |
Chitnis |
01:45:09 |
colourless cloudy |
History List
| Holder |
Time |
Name |
ExpNo |
Experiment |
User |
Load |
Atma |
Spin |
Lock |
Shim |
Acq |
Proc |
Title |
Remarks |
| 55 |
22:37:44 |
PT-077_2-after1wash-Dioxane |
4 |
1d_13C_UDEFT |
Chitnis |
- |
- |
- |
- |
- |
+ |
- |
colourless cloudy |
| 55 |
20:56:51 |
PT-077_2-after1wash-Dioxane |
3 |
1d_13C{1H} |
Chitnis |
- |
+ |
- |
- |
- |
+ |
+ |
colourless cloudy |
| 55 |
20:33:19 |
PT-077_2-after1wash-Dioxane |
1 |
1d_31P{1H} |
Chitnis |
- |
+ |
- |
- |
- |
+ |
+ |
colourless cloudy |
| 55 |
20:12:59 |
PT-077_2-after1wash-Dioxane |
2 |
1d_1H_HSolv |
Chitnis |
+ |
+ |
- |
+ |
+ |
+ |
+ |
colourless cloudy |
| 54 |
17:14:19 |
PT-083_2-air_3d-Dioxane |
1 |
1d_31P{1H} |
Chitnis |
+ |
+ |
- |
+ |
+ |
+ |
+ |
clear colourless (the vial is foggy) |
| 9 |
14:14:45 |
MAL-NacNacP-xtals |
2 |
1d_1H_HSolv |
MacDonald |
- |
+ |
- |
- |
- |
+ |
+ |
NacNacP-Na-THF supernate - orange solution THF / pentane, crystals grew in this, but brown NaPH2 goo at bottom removed |
| 9 |
13:54:40 |
MAL-NacNacP-xtals |
1 |
1d_31P{1H} |
MacDonald |
+ |
+ |
- |
+ |
+ |
+ |
+ |
NacNacP-Na-THF supernate - orange solution THF / pentane, crystals grew in this, but brown NaPH2 goo at bottom removed |
| 6 |
13:23:40 |
L1GA188001-1-1-b_MeOD |
1 |
1d_1H_Dsolv |
SSPI |
+ |
- |
- |
+ |
+ |
+ |
+ |
|
| 5 |
13:04:45 |
L1GA188001-79-1-b_MeOD |
1 |
1d_1H_Dsolv |
SSPI |
+ |
+ |
- |
+ |
+ |
+ |
+ |
|
| 3 |
12:39:09 |
Burke-xii-32 dmso |
1 |
1d_1H_HSolv |
Speed |
+ |
+ |
- |
+ |
+ |
+ |
+ |
|
| 2 |
12:31:59 |
Burke-xii-30b hex |
1 |
1d_1H_Dsolv |
Speed |
+ |
+ |
- |
+ |
+ |
+ |
+ |
|
| 1 |
12:25:26 |
Burke-xii-35 al2 |
1 |
1d_1H_HSolv |
Speed |
+ |
+ |
- |
+ |
+ |
+ |
+ |
|
